Thanks again Adam. The Rex Allers article suggests obtaining a hydrometer to monitor the density of the etchant, which should start out at a density of 1.17 g/mL, and will increase as copper dissolves into the solution. He suggests a hydrometer with an expanded scale of 1.15 to 1.25 g/mL. According to my tentative understanding a range of 19 to 31 Baume would work here, does this seem right? I note that American Science and Surplus has some Chinex lab glassware (student grade) at low prices. The beaker and erlenmeyer flasks are available in the sizes you suggest: http://www.sciplus.com/category.cfm?subsection=4 Would any of their pipettes do the trick? The Rex Allers article shows titration using the burette and beaker, is the erlenmyer flask better in some way? Grant --- In Homebrew_PCBs@...m, adam Seychell <adam_seychell@y...> wrote: > No reason I can think of. picnic coolers are cheap, and have a good lid. I built > my tanks because I needed those dimensions. I coudnl't find anything off the > shelf that was narrow and deep enough, base = 45x250mm high = 350 mm. > Any of the food plastics are ok with strong acids. > Now you only concern is getting hold of some lab equipment. > > Here is lab order list. > > 1 * 5 ml class B volumetric pipette > (preferred to graduated pipette) > (buy a second in case you break it) > 1 * rubber bulb pipette sucker > 1 * 125 ml dropper bottle for indicator (makes life easier) > 1 * 50 ml glass burette, class B. > 1 * 0-50°C (or 0-100°C) glass thermometer > 1 * 250 ml erlenmeyer flask > 1 * Bromophenol Blue indicator > (1 gram will last you ever and a day) > > > You also have to make some kind of stand to hold the burette, I made something > out of wood that was a *LOT* cheaper than buying a dedicated stand. Fasten the > burette with rubber bands to a length of wood, and hold that by a stand from a > heavy base using a diagonal pole. The area under the burette nozzle needs to be > free to place the erlenmeyer flask. > > The deionized water and sodium hydroxide is available from most supermarkets. > You also need some ethanol to make up the bromophenol blue indicator. Its > probably better to get the right indicator rather trying to use turmeric power > because it will be easier to see the end point of the titration, which makes the > job easier to carry out.
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Re: Cupric Choride etching - costs and benefits
2003-03-10 by grantfair2001
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