Note that H2O2 is photo-sensitive, and should be stored in a light-proof container. It will break down over time all by itself. You don't need a *lot* of H2O2 to etch, so a 3% solution is enough if you use the 2:1 ratio. The stronger H2O2 can be used a little at a time to "freshen" the etchant just before you use it. When I made my etchant, after I used it for circuit boards, I put about half a pound of solid copper in it (3-4 liters of etchant) and let it slowly dissolve, which gave me enough CuCl for the next etch. It took a while but eventually worked. Once it's converted to a CuCl etchant, you can refresh it with plain old air.
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Re: [Homebrew_PCBs] Observations on CuCl2 etching
2014-05-13 by DJ Delorie